法医学杂志

法医学杂志 ›› 1994, Vol. 0 ›› Issue (4): 0-0.

• 论文 •    

GC/MSD分析生物样品中的巴比妥类药物

曾苏   

  1. 淅江医科大学药物分析教研室
  • 发布日期:1994-08-25 出版日期:1994-08-28

Analysis of Barbiturates in Biological Specimen by GC/MSD

ZENG SU (DEPARTMENT OF DRUG ANALYSIS, ZHEJIANG MEDICAL UNIVERSITY;HANZHOU 310031)   

  • Online:1994-08-25 Published:1994-08-28

摘要： 本文建立了ＧＣ／ＭＳＤ分析生物样品中五种巴比妥类药物的测定方法。线性范围是２００～５０００ｎｇ／ｍｌ，方法的回收率：巴比妥８１．４１±４．５０；异戊巴比妥８３．５８±６．６５；戊巴比妥８２．７８±７．１７；司可巴比妥７９．０４±７．２０；苯巴比妥８２．１３±６．８１（ｎ＝６）。

关键词: 巴比妥类, GC／MSD

Abstract: This paper described the analytical method for five barbiturates in biological specimen by Gc/MDS. The linear ranges were 200-5000ng/ml and recoveries of the method are 81. 41±4. 50 for Barbital, 83. 58±6.65 for Amobarbital, 82. 78±7. 17 for Pentobarbital,79. 04±7. 20 for Secobarbital, 82. 13±6. 81 for Phenobarbital.

Key words: Barbiturates, biological specimen, GC/MSD, Analytical method