法医学杂志

法医学杂志 ›› 1994, Vol. 0 ›› Issue (4): 0-0.

• 论文 •    

酶水解后同时分析海洛因、吗啡、可待因

向平，沈保华   

  1. 司法部司法鉴定科学技术研究所
  • 发布日期:1994-08-25 出版日期:1994-08-28

SIMULTANEOUS ANALYSIS OF CODEIN,MORPHINE AND HEROIN AFTER GLUCURONIDASE HYDROLYSIS

XIANG PING; SHEN BAOHUA (INSTITUTE OF FORENSIC SCIENCES, MINISTRY OF JUSTICE; SHANGHAI 200063)   

  • Online:1994-08-25 Published:1994-08-28

被引次数

2

摘要： 本文以家兔为模型，用酶水解、丙酸酐衍生化处理吸毒后的尿样，用ＧＣ／ＭＳ同时分析海洛因、吗啡、可待因。

关键词: 酶水解, β—葡萄糖醛酸酶, 海洛因, 丙酸酐, 衍生比

Abstract: The method of simultaneous analysis of codein, morphine and 6-MAM and heroin by GC/MS is presented in this paper. The urine sample of toxic rabbit is extracted with chloroform: isopropanol (9:1) following enzyme hydrolysis. The residue is derived with propionic anhydride.

Key words: hydrolysis, B-glucuronidase, heroin, propionic anhydride, derivation.