氟乙酰胺和氟乙酸的毛细管柱气相色谱检测

法医学杂志 ›› 1997, Vol. 0 ›› Issue (2): 77-78+1.

氟乙酰胺和氟乙酸的毛细管柱气相色谱检测

员克明,王玉瑾,李贵明,王英元

山西医科大学法医学系!山西太原,030001,山西医科大学法医学系!山西太原,030001,山西医科大学法医学系!山西太原,030001,山西医科大学法医学系!山西太原,030001

发布日期:1997-04-25 出版日期:1997-04-28

Determination of fluoroacetatamide and fluoroacetic acid by capillary gas chromatography

　YUN KEMING; WANG YUJIN;LI GUIMING AND WANGYENGYUAN(DEPARTMENT OF FORENSIC MEDICINE,SHANXIMEDICAL UNIVERSITY, TAYUAN 030001)

Online:1997-04-25 Published:1997-04-28

摘要/Abstract

摘要： 本文建立氟乙酰胺和氟乙酸的毛细管柱气相色谱检测方法，氟乙酰胺和氟乙酸的线性检测范围为0．0625mg/ml～4mg／ml和0．625mg／ml~20mg／ml，最小检出浓度为31．25ug／ml和625ng/ml．太原地区地摊所售鼠药87．5％含有氟乙酰胺，30％含有氟乙酸．

关键词: 氟乙酰胺, 氟乙酸, 毛细管柱气相色谱

Abstract: A rapid qualitative and quantitative analysis offluoroacetatamide and fluoroacetic acid in rodenticides by capillary gaschromatography wasdescribed in this paper.lsoamyl alcohol was used asthe internal standard.The determination curves offluoroacetatamide and fluoroacetic acid inrodenticides were linear in the ranges of 0.06254mg/ml and 0.625-20mg/ml.The detection limits offluoroacetatamide and fluoroacetic acid were31.25ug/ml(32.5ng) and 625ug/ml (625ng). 87.5%and 30% of rodenticides sold in Taiyuan groundmarket from May.1995 to May.1996 containfluoroacetatamide and fluoroacetic acid.

Key words: fluoroacetatamide, fluoroacetic acid, GC

员克明;王玉瑾;李贵明;王英元. 氟乙酰胺和氟乙酸的毛细管柱气相色谱检测[J]. 法医学杂志, 1997, 0(2): 77-78+1.

　YUN KEMING;WANG YUJIN;LI GUIMING AND WANGYENGYUAN(DEPARTMENT OF FORENSIC MEDICINE;SHANXIMEDICAL UNIVERSITY;TAYUAN 0000). Determination of fluoroacetatamide and fluoroacetic acid by capillary gas chromatography[J]. , 1997, 0(2): 77-78+1.

[1]	宋爱英, 赵翌博, 杨利君. 液相色谱-串联质谱法检验氟乙酸致死1例[J]. 法医学杂志, 2023, 39(4): 428-430.
[2]	封世珍;于忠山. GC/NPD、GC/FID分析生物样品中的氟乙酰胺[J]. 法医学杂志, 1999, 0(2): 0-0.
[3]	褚建新;满勤;朱军. 硫靛反应检验氟乙酰腔的方法研究[J]. 法医学杂志, 1998, 0(4): 220-222.