法医学杂志 ›› 1988, Vol. 0 ›› Issue (2): 29-33+4.

• 论文 • 上一篇    下一篇

毒鼠磷中毒检验的实验研究 Ⅱ、毒鼠磷的定性定量分析

沈敏;吴侔天;卜俊;   

  1. 司法部司法鉴定科学技术研究所,司法部司法鉴定科学技术研究所,司法部司法鉴定科学技术研究所,
  • 发布日期:1988-04-25 出版日期:1988-04-28

Experimental Study on Detection Methods of Phosacetim in Intoxicant Death Ⅱ. Qualitative and Quantitative Analysis of Phosacetim in Biological Samples

SHEN MIN;WU MOUTIAN;BU JUN DEPARTMENT OF FORENSIC CHEMISTRY, INSTITUTE OF FORENSIC SCIENCES, MINISTRY OF JUSTICE, PRC   

  • Online:1988-04-25 Published:1988-04-28

摘要: <正> 毒鼠磷中毒的检材采取及预处理问题,己在“毒鼠磷中毒检验的实验研究—Ⅰ”文中作了讨论。本文研究采用薄层层析(TLC)、薄层扫描(TLCS)、高效液相色谱(HPLC)等方法定性定量分析生物体内的毒鼠磷,取得较为满意的结果。这些方法简便、灵敏、重现性较好。且薄层色谱法和高效液相色谱法间具有良好的相关性,r=0.996。方法适合于毒鼠磷中毒案的检验。

Abstract: This paper describes the methods for qualitative and quantitative analys- is of phosacetim in biological samples by TLC, TLCS and HPLC. The methods given are quick, reproducible and linear with correlation coefficient of TLC and HPLC was 0. 996. The presence of interfering components, as are com- monly found in postmortem, did not affect the result. For these reasons, the methods were well suited for the analysis of phosacetim in the forensic laboratory.