法医学杂志 ›› 1993, Vol. 0 ›› Issue (3): 97-102+.

• 论文 •    下一篇

气-质联用法(EI.PCI.NCI)在系统毒物分析中的应用

沈敏;孙亚娟;沈保华;向平;严伟民;张玉荣;   

  1. 司法鉴定科学研究所,司法鉴定科学研究所,司法鉴定科学研究所,上海市公安局刑料所,上海市公安局刑料所,上海市公安局刑料所 上海:200063,上海:200063,上海:200063
  • 发布日期:1993-06-25 出版日期:1993-06-28

Application of Gas Chromatography/Electron Impact (EI),Positive—ion Chemical Ionization (PCI)and Negative—ion Chemical Ionization (NCI)Mass spectrometry in Systematic Analytical Toxicology

SHEN MIN SUN YAJUAN SHEN BAOHUA XIANG PING YAN WEIMIN ZHANG YURONG INSTITUTE OF FORENSIC SCIENCES,MINISTRY OF JUSTICE,PRC;SHANGHAI CHINA(200063)   

  • Online:1993-06-25 Published:1993-06-28

摘要: 本文应用电子轰击质谱(EI),正、负化学电离质谱(PCI.NCI)技术,建立了315种常见毒,药物的气一质联用系统分析方法。并建立了 EIMS、PCIMS、NCIMS 质谱图谱库。司法鉴定实践表明使用气相保留指数,特征碎片和 EI、PCI、NCI 图谱库检索等多指标的系统分析方法,是未知物鉴定的强有力的工具。

关键词: 气-质联用, 正, 负化学电离质谱, 系统毒物分析

Abstract: A systematic identificattion sysytem was developed for the simultaneous analysis 315 abuse drugs amd poisons by GC/MS(EI、PCI、NCI).The paper also presented EI、PCI and NCI mass spectra data library of 315 drugs and poisons.The forensic sciences practice demonstrated that the systematic analysis using multiple parameters:GC retention indices,typicalions and EI,PCI and NCI spectrum matching would be a powerful tool in the identificattion of unkonow compound.

Key words: GC/MS, PCI and NCI MS, Systematic Analytical Toxicology