法医学杂志

法医学杂志 ›› 1994, Vol. 10 ›› Issue (1): 0-0.

• 论文 •    

水、尿、血中苯类化合物的顶空色谱分析

孙亚娟，黄仲杰，沈保华，向平   

  1. 司法部司法鉴定科学技术研究所
  • 发布日期:1994-02-25 出版日期:1994-02-28

DETERMINATION OF BENZENE SERIES IN WATER,URINE,BLOOD USING HEAD-SPACE GAS CHROMATOGRAPHY

SUN YAJUAN, HUANG ZHONGJIE, SHEN BAOHUA, XIANG PING. (INSTITUTE OFFORENSIC SCIENCES, MINISTRY OF JUSTICE, SHANGHAI, CHINA200063).   

  • Online:1994-02-25 Published:1994-02-28

被引次数

6

摘要： 本文报道用顶空气相色谱，ＦＩＤ检测器，８０／１２０目Ｃａｒｂｏｐａｃｋ／５％Ｃａｒｂｏｗａｘ２０Ｍ２ｍ×２ｍｍ玻璃填充柱分离筛选及测定水、血、尿中苯类化合物的方法．叔丁醇作内标．检测限为０．１～０．０５μｇ／ｍｌ．该方法灵敏度高，快速、简便．适用于苯类化合物中毒案例的测定．

关键词: 顶空, 气相色谱法, 苯, 甲苯, 乙苯, 二甲苯

Abstract: Abstract: A head-space method for the deteminatiou ofbenzene, toluene. ethy1 benzene and dimethy1 benzene inwater, urine or blood using a GC with a FID was devel oped. Internal standard were Tertiary Buty1 Alcohol.Glass cotumn packed with 80-120 mesh carbopack / 5% carbowax 20M. The detection limit was 0.1-0.05μg/ml.This method is sensitive, simple and rapid. it is useful in analitical toxicology.