法医学杂志

法医学杂志 ›› 2006, Vol. 0 ›› Issue (4): 285-287.

• 论文 • 上一篇    下一篇

东莨菪碱的GC/MS检验

褚建新;谢瑜;卓晓聪;   

  1. 浙江省人民检察院,杭州市萧山区公安分局,杭州市萧山区公安分局 浙江杭州310012,浙江杭州311200,浙江杭州311200
  • 发布日期:2006-08-25 出版日期:2006-08-28

Determination of Scopolamine in the Poisoning Case by GC/MS

CHU JIAN-XIN1, XIE YU2, ZHUO XIAO-CONG2 (1. THE PROCURATORATE OF ZHEJIANG PROVINCE, HANGZHOU 310012, CHINA; 2. XIAOSHAN BRANCH OF HANGZHOU PUBLIC SECURITY BUREAU,HANGZHOU 311200, CHINA)   

  • Online:2006-08-25 Published:2006-08-28

被引次数

5

摘要： 目的用气质联用方法分离定性案件检材中微量的东莨菪碱成分。方法以液-液萃取法提取分离,用CP5860(CP-sil8CB)毛细管拄(30m×0.25mm×0.33!m),并采用气质联用仪(GC/MS)测定东莨菪碱。结果可检出检材中微量东莨菪碱,色谱分离良好。结论以气质联用仪(GC/MS)测定东莨菪碱方法灵敏度高,测定结果准确可靠。

关键词: 东莨菪碱, 中毒, GC/MS

Abstract: Objective To separate and determine scopolamine from the food in a poisoning case by GC/MS. Methods The scopolamine was determined by GC/MS/EI used CP5860(CP-sil8CB) column (30 m×0.25 mm×0.33 ?滋m) with liquid- liquid extraction. Results The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine. Conclusion The method is accurate and reliable.

Key words: scopolamine, Poisoning, GC/MS